
V2+ is oxidised in air, therefore to observe the V2+, the test tube may need a stopper once the reduction has begun. Otherwise it turns back green because of its contact with oxygen in the air. It is oxidised back to vanadium(III).
What do you observe as ammonium vanadate(V) is reduced?
Answer:
The solid dissolves in the acid to form a yellow solution. This becomes a blue, then green and finally violet solution
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